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To prepare a 0.1 N sodium oxalate (Na2C2O4) solution, first calculate the required mass by using the formula: mass (g) = normality (N) × equivalent weight (g/equiv) × volume (L). The equivalent weight of Na2C2O4 is 126.07 g/mol divided by 2, since it can donate two moles of oxalate ions (C2O4^2-), resulting in 63.035 g/equiv. Weigh out the appropriate mass of Na2C2O4, dissolve it in distilled water, and then dilute to the desired final volume, ensuring thorough mixing.

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